Msbauer spectroscopic study on the amorphous Fe-Zr-B films

CHENG Xinli1  XU Yusheng2  XU Weixin3  JIN Huijuan3 1

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Msbauer spectroscopic study on the amorphous Fe-Zr-B films

更新时间：2021-03-12

- Msbauer spectroscopic study on the amorphous Fe-Zr-B films
- NUCLEAR TECHNIQUES Issue 2, (2003)
- 作者机构：
  
  1. 中国科学院上海微系统与信息技术研究所
  2. 苏州大学物理科技学院,上海,200050
  3. ,苏州,215006
- 作者简介：
- 基金信息：
- DOI：
  CLC： O484
- Published：01 February 2003
- 稿件说明：
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[1]程新利,许裕生,徐炜新,金慧娟.非晶Fe-Zr-B薄膜穆斯堡尔谱学研究[J].核技术,2003(02):146-150.

CHENG Xinli1 XU Yusheng2 XU Weixin3 JIN Huijuan3 1. Msbauer spectroscopic study on the amorphous Fe-Zr-B films[J]. Nuclear techniques, 2003, (2): 146-150.
[1]程新利,许裕生,徐炜新,金慧娟.非晶Fe-Zr-B薄膜穆斯堡尔谱学研究[J].核技术,2003(02):146-150. DOI：

CHENG Xinli1 XU Yusheng2 XU Weixin3 JIN Huijuan3 1. Msbauer spectroscopic study on the amorphous Fe-Zr-B films[J]. Nuclear techniques, 2003, (2): 146-150. DOI：

摘要

用X射线衍射分析、X射线光电子能谱（XPS）和穆斯堡尔谱学研究了直流磁控溅射法制备的Fe-Zr-B薄膜。X射线衍射分析结果表明制备态的薄膜是非晶的;X射线光电子能谱（XPS）结果表明样品表面氧化较明显

深层部分Fe

B结合占主导地位;穆斯堡尔谱学结果表明薄膜中Fe原子周围Zr、B原子的存在使Fe原子核内场值有所下降并导致超精细场分布P（H）出现双峰结构

薄膜中存在两种不同的局域微结构。

Abstract

The amorphous Fe-Zr-B films prepared by DC magnetron sputtering have been studied using X-ray dif-fraction

XPS and Msbauer spectroscopy

and compared with amorphous ultrafine Fe-Zr-B powder prepared by chemical reduction. The XPS shows that surface of the film is oxidized partly

the interactions among Fe

B are strong in deeper part. The result of Msbauer spectroscopy shows that Zr and B atoms around Fe atoms cause the re-duction of hyperfine field at Fe nucleus and make the distribution of magnetic hyperfine field with two peaks. This implies that the amorphous Fe-Zr-B film consists of two amorphous microstructures.

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Enhanced mechanical properties and corrosion resistance of Zr-based amorphous/crystalline nuclear material

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